论文摘要
b-FeOOH nanorods were prepared by a poly ethylene glycol（PEG） assisted precipitation of FeCl3·6 H2O aqueous solution with urea. Na2CO3 aqueous solution was introduced to maintain their shapes under annealing. The one-dimensional porous iron oxide nanorods were synthesized successfully. The asprepared catalysts were characterized by X-ray diffraction, transmission electron microscopy, N2 adsorption-desorption isotherms and X-ray photoelectron spectroscopy. The hydrogenation of nitrobenzene to aniline was taken as probe reaction to evaluate their catalytic performance. FeOOH（iron oxides hydroxide） nanorods, fabricated by annealing b-FeOOH nanorods at 250℃ in Ar atmosphere for 4h, exhibited high catalytic activity for the transfer hydrogenation of nitrobenzene to aniline with hydrazine hydrate as hydrogen donors.
论文目录
文章来源
类型: 期刊论文
作者: Yanshuang Ma,Liyun Zhang,Wen Shi,Yiming Niu,Bingsen Zhang,Dangsheng Su
来源: Chinese Chemical Letters 2019年01期
年度: 2019
分类: 工程科技Ⅰ辑
专业: 化学
单位: Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences,School of Materials Science and Engineering, University of Science and Technology of China
基金: the financial support provided by the National Natural Science Foundation of China (Nos. 91545119,21761132025,21773269,21703262,and 51521091),Youth Innovation Promotion Association CAS (No. 2015152),“Strategic Priority Research Program” of the Chinese Academy of Sciences (No. XDA09030103)
分类号: O643.36;O625.631
页码: 183-186
总页数: 4
文件大小: 2874K
下载量: 20